Course Information
Course Title Code Semester T + P ECTS
Instrumental Analysis KIM321 5 4 + 0 6

Prerequisites none

Language Turkish
Level Bachelor's Degree
Type Compulsory
Coordinator Prof. MAHMUT KÖSE
Instructors Prof. MAHMUT KÖSE
Goals The aim of this course is to provide the fundamentals and analytical applications of instrumental methods such as chromatographic techniques; spectroscopic techniques; thermal methods.
Contents Ultraviolet/visible absorption spectroscopy (UV-VIS) Molecular fluorescence and chemiluminescence spectroscopy Infrared Spectroscopy (FT-IR) Nuclear magnetic resonance spectroscopy (NMR) Nuclear magnetic resonance spectroscopy (NMR) Mass spectroscopy Electroanalytical chemistry Atomic Spectroscopy Chromatographic Methods: (Liquid chromatography, Glass column chromatography, Thin layer chromatography (TLC), Ion-exchange chromatography, High-performance liquid chromatography (HPLC) Gas Chromatography (GC) Polarimetry; Refractometry Thermal methods
Work Placement(s) Absent

Number Learning Outcomes
1 At the end of the course the student will be able to: Classify the instrumental analysis techniques
2 Understand working principleof instruments use in chemistry
3 Interpret experimental data obtained from spectroscopic methods used in characterizing organic compounds
4 Perform and justify the separation techniques used in purifying organic compounds
5 Select the type of technique in the analysis of an unknown sample

Mode of Delivery Face-to-Face
Planned Learning Activities & Teaching Methods Lecture, Discussion, Question & Answer, Demonstration, Drill - Practise
Assessment Methods Midterm Exam, Final Exam



Course Content
Week Topics Study Materials
1 Introduction to Instrumental Analysis [1] Chapter I: Introduction to Instrumental Analysis (Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
2 Ultraviolet/visible absorption spectroscopy (UV-VIS) [1] Chapter 2: Ultraviolet/visible absorption spectroscopy (UV-VIS)(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
3 Molecular fluorescence and chemiluminescence spectroscopy [1] Chapter 3: Molecular fluorescence and chemiluminescence spectroscopy(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
4 Infrared Spectroscopy (FT-IR) [1] Chapter 4: Infrared Spectroscopy (FT-IR)(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
5 Nuclear magnetic resonance spectroscopy (NMR) [1] Chapter 5: Nuclear magnetic resonance spectroscopy (NMR)(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
6 Nuclear magnetic resonance spectroscopy (NMR) [1] Chapter 6: Nuclear magnetic resonance spectroscopy (NMR)(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
7 Mass spectroscopy [1] Chapter 7: Mass spectroscopy(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
8 Electroanalytical chemistry [1] Chapter 8: Electroanalytical chemistry(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
9 Mid-terms exam
10 Atomic Spectroscopy [1] Chapter 9: Atomic Spectroscopy(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
11 Chromatographic Methods: (Liquid chromatography, Glass column chromatography, Thin layer chromatography (TLC), Ion-exchange chromatography, High-performance liquid chromatography (HPLC) [1] Chapter 10: Chromatographic Methods(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
12 Gas Chromatography (GC) [1] Chapter 11: Gas Chromatography (GC)(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
13 Polarimetry; Refractometry [1] Chapter 12: Polarimetry; Refractometry(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)
14 Thermal methods [1] Chapter 13: Thermal methods(Enstrümantal Analiz I Ders notları, Prof. Dr. Mahmut Köse)



Sources
Textbook 1. Lecture notes of Instrumental Analysis I, by Prof. Dr. Mahmut Köse 2. İnstrümental Analiz, Prof. Dr. Turgut GÜNDÜZ, Gazi Kitapevi, 6. Baskı, 2002
Additional Resources 3. Enstrümantal Analiz, Skoog, Holler and Nieman, 7. Baskıdan çeviri, (Çeviri Editörleri: Esma Kılıç, Fitnat Köseoğlu ve Hamza Yılmaz), Bilim yayıncılık, Ankara 4. Introduction to Organic Spektroscopy, L. M. Harwood and T. D. W. Claridge, Oxford University Press, 1997. 5. Spectroscopic Methods in Organic Chemistry, D. H. Williams and I. Fleming, Fifth Edition, McGRAW-HILL BOOK COMPANY, London,1995. Organik Kimyada Spektroskopik Yöntemler, prof. Dr. Ender Erdik, (2. Baskı), Gazi Kitapevi, Ankara, 1998. 6. Organic Spectroscopy, (Second edition), William Kemp,MACMILLAN EDUCATION LTD, London, 1987 7. Nükleer Manyetik Rezonans Spektroskopisi, Prof. Dr. Metin Balcı, (2. Baskı), ODTÜ yayıncılık, 2004.



Assessment System Quantity Percentage
In-Term Studies
Mid-terms 1 100
In-Term Total 1 100
Contribution of In-Term Studies to Overall 40
Contribution of Final Exam to Overall 60
Total 100





Course's Contribution to PLO
No Key Learning Outcomes Level
1 2 3 4 5
1 Has textbooks containing current information, application tools and equipment , and advanced theoretical and practical knowledge supported by other resources in a scientific approach. x
2 Adapts and transfers the acquired knowledge to secondary education. x
3 Uses advanced institutional and practical knowledge acquired in the field. x
4 Updates the information on daily conditions. x
5 Comments on and evaluate the data by using advanced knowledge and skills acquired in the field, identifies and analyzes the current problems of technological developments, and comes up with solutions based on research and evidence. x
6 Has the ability to conceptualize the events and facts related with the field; analyze them with scientific methods and techniques. x
7 Designs and performs experiments to analyze the problems, collects data, performs analyzes and comment on the results. x
8 Carries out an advanced study related to the field independently. x
9 Takes on responsibility individually and as a team member in order to solve unpredictable and complex problems encountered in applications related to the field. x
10 Plans and manages the activities in a project under his responsibility for development. x
11 Plays a role in the process of decision making when faced with problems about different discipline fields. x
12 Uses time effectively in the process of inference with the ability of thinking analytically. x
13 Evaluates the advanced knowledge and skills acquired in the field with a critical perspective. x
14 Determines the learning requirements and leads the learning process. x
15 Develops a positive attitude towards lifelong learning. x
16 Is aware of the necessity of lifelong learning and develops his Professional knowledge and skills continuously. x
17 Informs people and organizations about the topics related to their fields; expresses his ideas and suggestions for solutions to problems in both oral and written form. x
18 Shares his ideas and suggestions for solutions to the problems with experts and non-experts by supporting them with quantitative and qualitative data. x
19 Organizes projects and activities for social environment he lives in with an awareness of social responsibility. x
20 Follows advances in the field and communicate with colleagues by using a foreign language at least at B1 level of European Language Portfolio. x
21 Uses information and communication technology along with software the Human Sciences the field requires at an advanced level. x
22 Uses his knowledge of human health and environmental awareness acquired in their fields for society’s ends. x
23 Behaves in a way adhering to the social, scientific, cultural and ethical values in the process of data collection, commenting, application, publicizing the results related with the field x
24 Has a sufficient level of awareness about the universality of social rights, social justice, quality management, acting in a suitable way in processes and attendance (Instead of quality culture) the protection of cultural values, protection of the environment and health and security in the professional field. x



ECTS ALLOCATED BASED ON STUDENT WORKLOAD BY THE COURSE DESCRIPTION
Activities Quantity Duration (Hour) Total Work Load (h)
Course Duration 14 4 56
Hours for off-the-classroom study (Pre-study, practice) 14 5 70
Mid-terms 1 25 25
Final examination 1 30 30
Total Work Load (h) 181
Total Work Load / 30 (h) 6.03
ECTS Credit of the Course 6